Have you ever run flash column chromatography with mass detection flashms and observed the total ion current or tic increase during the purification only to find that there was no discernible compound contributing to the effect. Biotage initiator cavity air guide fisher scientific. In addition to the standard 1point support provided to all biotage customers, as described in detail below, you can purchase extended warranty plans for each product, or broad support plans for your entire array of biotage systems. How to use biotage snap ultra cartridges on combiflash rf systems page 1 of 2 how to use biotage snap ultra cartridges on combiflash rf systems a quick guide biotage snap ultra cartridges are compatible with combiflash rf systems. More relevant content may be added as customer demand increases. Speeding up automated flash purification what is biotage isolera anyway. The biotage sp1 is a stateoftheart flash chromatography system used to purify compounds in an accelerated manor. Peptide chemists are now incorporating our novel evaporation technology in their workflow, to rapidly evaporate aqueous and organic solvents with boiling points from 30 c to 205 c. Biotage ab and mcmaster university sign two year extension. The sp1 flash purification system comes equipped with a builtin windows based control computer and an intuitive touch screen controller that allows a simple three step process to run a sample.
Silicon carbide passive heating elements in microwave. Biotage offers a wide range peptide synthesizers for fmoc solid phase peptide synthesis. Transferring reacted materials from a microwave synthesizer to dried vial is easy with the liquid handler. The modular design allows a user to add on different automated sample processors dependent on throughput requirements. This tutorial video outlines the system components, controls, and how a chromatography run is set up. Biotage ab and mcmaster university sign two year extension to molecular imaging development agreement. Biotage is a leading global company in the chemical synthesis field with numerous customers in the pharmaceutical, biotech and food industries as well as a large number of academic and scientific institutions. Supplier name supplier part number mfrr name item description uom published price biotage 00000001 biotage fm personal fittings kit each 56 biotage 00000011 biotage flashpack module lue900410r biotage product part list official gimitec website.
Biotage 354974 this product was recently added by customer request, and is available for your convenience. Jun 11, 2018 biotage initiator microwave synthesizer with robot eight is available from the lab world group. Polysaccharide based surfactants as alternative to. Pioneers in flash chromatography and custom resins. Biotage introduces new flash cartridges for peptide. As a convenience, biotage snap ultra cartridges with luer slip connectors are. Add sample here central insert drain hole figure 1. Have you ever run flash column chromatography with mass detection flashms and observed the total ion current or tic increase during the purification only to find that there was.
Biotage ab and mcmaster university sign two year extension to. Oct 26, 2015 biotage announces the introduction of isolera assist, a new intelligent user experience for their flash purification systems. Microwave synthesizing done safe and fast with biotage initiator. Biotage microwave synthesizer, model initiator exp us with biotage initiator robot eight.
Note that the design allows for magnetic stirring of the reaction mixture during the reaction with a standard stir bar placed below the phe cylinder. Biotage microwave systems are predictable, reliable and safe. See who you know at biotage ab, sweden, leverage your professional network, and get hired. Biotage is a global life science company that develops innovative and effective solutions for separation within organic and analytical chemistry, as well as for industrial applications. Biotage microwave systems support a wide variety of different reaction. Used biotage initiator exp us 300w microwave synthesizer lab. This easy to use chromatograph includes features such as waste and solvent monitoring along with a builtin fraction collector. Used biotage sp 4 flash purification system lab general.
The intuitive initiator software controls the instrument functions and by using the. Mcmaster university has successfully completed the first year research agreement, with a key. Biotage microwave reactor is designed to enhance the ability to perform chemical reactions under controlled conditions on a laboratory scale. Removal will begin on july 25th by scheduled appointment only. I have been using the feature to create a gradient from tlc and have been loading the sample. Used biotage initiator exp us 400w microwave synthesizer. We strive to provide our customers with a onestop shop for the entire scientific supplies category. Semiautomated, which i think is ideal for an academic lab making lots of. This instruments highend specifications enable the chemist to explore new areas and perform the latest of innovations in chemistry. Biotage flash 400 industrial purification system on vimeo. Refurbished biotage initiator exp us microwave reactor.
The biotage universal phase separator is a simple solution to the classic problem of separating an upper organic phase from an aqueous during a traditional liquidliquid extraction. Polysaccharide based surfactants as alternative to nonylphenol ethoxylates in laundry detergents. Biotage microwave synthesizer, model initiator exp us with. We offer the most advanced products for flash chromatography, making purification faster, greener, and easier than ever before. Microwave reactor biotage materials research laboratory.
The biotage isolera one flash chromatograph brings you an advanced, fully automated compound purification in one compact package. Microwave reactor biotage materials research laboratory at. The biotage hpfc system passed all tests and was found. Used biotage initiator exp us 400w microwave synthesizer pred. The initiator is upgradeable from the singlesample manual format to. The biotage vacmaster disk is a solid phase extraction system for performing manual, diskbased extractions. Biotage introduces isolera assist, a new simple to use flash purification interface. The company is headquartered in uppsala, sweden, with offices in china, japan, the united kingdom, the united states and a worldwide network of distributors.
Allow me, however, to tell you about a column chromatography method that is very powerful. The solutions we offer include sample preparation, synthesis, workup and purification, which includes the argonaut. Biotage introduces biotage snap ultra high performance. This flash chromatograph features a variable uv wavelength detector with a range between 200400 nm. Biotage summer program at the university of richmond. The latest generation of microwave synthesis systems are compact. With functionality such as branches, preactivation and edit on the fly, and options for uv monitoring and maos organic synthesis capability, this instrument represents bestinclass systems for both small and large scale synthesis of peptides, peptoids, pna and peptidomimetics. The biotage initiator exp us microwave reactor synthesis system w robot eight is an entrylevel system for standard routine synthesis. Biotage zip cartridges are packed with biotage kpsil brand silica. This video starts with a wide shot of the biotage initiator exp us 400w microwave synthesizer. Dehydration of disaccharides and polysaccharides in biphasic amberlyst38kbraqgvl system. The system can easily be upgraded from a singlesample manual format to an automated.
How to use biotage snap ultra cartridges on combiflash rf systems. Available in sizes from 5120 g, biotage zip cartridge purifications can be directly scaled up to larger biotage cartridges including biotage snap 340 g, 750 g and 1500 g formats. Then we zoom in on the the initiator and view the about screen. Biotage isolera prime, biotage isolera one, biotage isolera four, and biotage isolera ls large scale. Biotage v10 touch demo part 8 of 8 drying down from. Does anyone have experience with biotage isolera sample. Biotage first pioneered prepacked purification columns back in the 1970s. Biotage v10 touch rapidly dries samples dissolved in both aqueous and organic solvents. Scroll up or down through the text when a help window has more than one. Semiautomated, which i think is ideal for an academic lab making lots of bizarre peptides and. Biotage initiator exp us 300w microwave synthesizer w robot sixty instrument only. All reagents and solvents were obtained from commercial sources and used without further purification.
Biotage sp 4 chromatography hpfc flash purification system pred. Biotage competitors and products in the pharmaceutical. In the presence of a 2 cm magnetic stir bar, efficient stirring is possible. Biotage initiator tm microwave heating specification. Biotage introduces isolera assist, a new simple to use. Biotage announces the introduction of isolera assist, a new intelligent user experience for their flash purification systems. It is an upgradeable and reliable platform allowing chemists to make great discoveries in less time. Samplets are placed inside of biotage snap cartridges which maximizes the amount of media available for purification and eliminates and precipitation risk. Biotage initiator eight microwave synthesizer is the newest addition to the initiator family, designed to provide medicinal chemists with the level of automation they need when performing microwaveassisted synthesis.
Biotage 440ez20 zip flash chromatography cartridge. Microwave chemistry is based on the efficient heating of materials by microwave dielectric heating effects. Biotage product part list official gimitec website. The biotage hpfc system passed all tests and was found to be. Biotagepersonal chemistry user group meeting 281004. The system is designed for high productivity laboratories and is an excellent first step for laboratories interested in moving from liquidliquid extractions to solid phase extractions for sample preparation. Biotage offers solutions, knowledge and experience in the areas of analytical and medicinal chemistry. Easily upgrade from a singlesample manual format to an automated. Biotage initiator eight from biotage selectscience. How to use biotage snap ultra cartridges on combiflash rf. Customers include the worlds top pharmaceutical and biotechnology companies, as well as leading academic institutes. Biotage introduces new flash cartridges for peptide purification. After evaporation of the solvent, dried adsorbent is poured into. Biotage magnetic stir bar, 25ml, pack of 25 mgntic sb 25 ml.
What im going to present today is likely familiar to our chemstation readers. Biotage introduces snap ultra high performance flash. Biotage summer program at the university of richmond reactions 1a. Practical microwave synthesis for organic chemists wiley online. Synthesis of pyridodiindoles with anticancer activity by a. Supplier name supplier part number mfrr name item description uom published price biotage 00000001 biotage fm personal fittings kit each 56 biotage 00000011 biotage flashpack module lue900410r tip asm. Biotage initiator microwave synthesizer with robot eight is available from the lab world group.
Used biotage initiator exp us 300w microwave synthesizer. The method uses the fact that different compounds have different. Mar 04, 2008 biotage ab and mcmaster university sign two year extension to molecular imaging development agreement. Biotage how do i remove an annoying ms tic background. The reactions were carried out in 5 ml glass tubes, sealed with microwave cavity. Set up the reaction contidions in less than a minute and youre good to go. Biotage is a worldwide supplier of instruments and consumables for analytical, organic and peptide chemistry. Each instrument has precise control of time, temperature and pressure to ensure that methods are.
Biotage initiator alstra getting started guide for peptide synthesis. Biotage flash 400 purifies 8 kg of product in one batch. Pioneers of flash purification biotage, pioneers of flash purification, have a proven record of innovation that began twenty years ago with the development of the first packed flash columns and first microprocessor controlled purification systems. The fisher scientific encompass program offers items which are not part of our distribution portfolio. This biotage sp4 chromatography hpfc flash purification system is in good functional condition. These products typically do not have pictures or detailed descriptions. The biotage sp1 flash chromatography system is small enough to fit on any lab bench, or even inside a standard fume hood. Biotage discovery chemistry groups mission is to be the preferred supplier of innovative highquality tools that work together to improve productivity for analytical chemists, medicinal chemists, and process development groups. Microwave irradiation experiments all microwave irradiation experiments were carried out in a biotage initiator. Manual addition of exact reagent amounts minimizes waste. Biotage magnetic stir bar, 25ml, pack of 25 mgntic sb 25. Does anyone have experience with biotage isolera sample loading. Biotage introduces isolera assist, a new simple to use flash.
625 875 1672 114 33 221 59 245 1160 1479 1293 1497 546 1108 490 1348 484 1382 246 1544 1527 359 1603 1133 161 1240 576 1269 131 813 1602 1524 319 352 919 367 89 1352 541 197 1296 1162 426 536